• 文献标题:   Determination of Aflatoxin B-1 and Aflatoxin B-2 in Edible Oil by Using Graphene Oxide-SiO2 as Soild Phase Extraction Coupled with HPLC
  • 文献类型:   Article
  • 作  者:   WANG HL, YU L, LI PW, LI M, ZHANG Q, ZHANG W
  • 作者关键词:   silica dioxide bound graphene oxide, solid phase extraction, aflatoxin, edible oil, high performance liquid chromatography
  • 出版物名称:   CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
  • ISSN:   0253-3820 EI 1872-2040
  • 通讯作者地址:   Chinese Acad Agr Sci
  • 被引频次:   4
  • DOI:  
  • 出版年:   2014

▎ 摘  要

Silica dioxide bound graphene oxide (GO-SiO2) was applied as an effective adsorbent for determination and quantiflcation of aflatoxin B-1, B-2 in edible oil by HPLC. The optimized conditions were GO-SiO2 0.15 g, extraction time 20 min, elution reagent acetonitrile, elution cycles two times. Results showed under the optimum conditions, the detection limits of aflatoxin B-1, B-2 were 0.17 and 0.05 mu g/L, respectively. The method was successfully applied to the detection of the actual edible oil, the spiked recoveries of aflatoxin B-1 and B-2 were 81.4%-105.3% and the relative standard deviations were 1.3%-8.6%.