• 文献标题:   A One Step Hydrothermal Approach for the Improved Synthesis of Graphene Nanosheets
  • 文献类型:   Article
  • 作  者:   KRISHNAMOORTHY K, VEERAPANDIAN M, KIM GS, KIM SJ
  • 作者关键词:   graphene nanosheet, hydrothermal approach, raman spectroscopy, xray photoelectron spectroscopy
  • 出版物名称:   CURRENT NANOSCIENCE
  • ISSN:   1573-4137 EI 1875-6786
  • 通讯作者地址:   Jeju Natl Univ
  • 被引频次:   8
  • DOI:   10.2174/157341312803989088
  • 出版年:   2012

▎ 摘  要

In this paper, we are reporting a one step hydrothermal approach to the synthesis of graphene nanosheets via reduction of graphene oxide (GO). The obtained graphene nanosheets are characterized using X-ray diffraction (XRD), UV-vis spectroscopy, Transmission electron microscope (TEM), X-ray photoelectron (XPS) and Raman spectroscopic techniques. XRD analysis revealed the re-graphitization process occurred in the graphene nanosheets. The UV-vis spectroscopy showed red shift in the absorption band due to the formation of graphene nanosheets. TEM studies revealed the sheet like morphology of the obtained graphene. XPS spectra confirmed the removal of oxygenated functional groups in graphene due to the hydrothermal reduction reaction. Raman spectra confirmed the restoration of sp(2) clusters in graphene sheets after the reduction. The average crystallite size of the sp 2 clusters in graphene sheets was calculated from the Raman spectra as 11.76 nm.