▎ 摘　　要

Nickel-graphene metal matrix composite coatings were fabricated by pulse electrodeposition technique from a Watt's type electrolyte. Effect of the graphene concentration in the electrolyte on the microstructure, microhardness, tribological features of nanocomposite coatings were evaluated in details. Microhardness of the composite coating was measured using a Vicker's microhardness indenter. The surfaces of the samples were characterized by scanning electron microscopy (SEM). Raman spectroscopy, EDS and XRD analysis were used to determine chemical composition and structure of composite coatings. The tribological behavior of the resultant composite coating was tested by a reciprocating ball-on disk method at constant load but varying sliding speeds for determination the wear loss and friction coefficient features against a counterface. The wear and friction variations of the electrodeposited nickel graphene nanocomposite coatings sliding against an M50 steel balls were carried out on a CSM Instrument. The friction and wear properties of the coatings were examined without any lubrication at room temperature in the ambient air. The change in wear mechanisms by changing graphene nanosheets content was also comprehensively studied. (C) 2015 Elsevier B.V. All rights reserved.