• 文献标题:   Synthesis of Water-Dispersed Sulfobetaine Methacrylate-Iron Oxide Nanoparticle-Coated Graphene Composite by Free Radical Polymerization
  • 文献类型:   Article
  • 作  者:   PERUMAL S, ATCHUDAN R, LEE YR
  • 作者关键词:   graphene composite, iron oxide nanoparticle, poly2 methacryloyloxy ethyldimethyl 3sulfopropyl ammonium hydroxide, sonication bath, thinlayered graphene
  • 出版物名称:   POLYMERS
  • ISSN:  
  • 通讯作者地址:  
  • 被引频次:   3
  • DOI:   10.3390/polym14183885
  • 出版年:   2022

▎ 摘  要

Research on the synthesis of water-soluble polymers has accelerated in recent years, as they are employed in many bio-applications. Herein, the synthesis of poly[2-(methacryloyloxy)ethyl]dimethyl-(3-sulfopropyl)ammonium hydroxide (PSB) by free radical polymerization in a sonication bath is described. PSB and iron oxide nanoparticles (IONPs) were simultaneously stabilized on the graphene surface. Graphene surfaces with PSB (GPSB) and graphene surfaces with PSB and IONPs (GPSBI) were prepared. Since PSB is a water-soluble polymer, the hydrophobic nature of graphene surfaces converts to hydrophilic nature. Subsequently, the prepared graphene composites, GPSB and GPSBI, were well-dispersed in water. The preparation of GPSB and GPSBI was confirmed by X-ray diffraction, Raman spectroscopy, field emission scanning electron microscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, and thermogravimetric analysis. The impacts of PSB and IONPs on the graphene surfaces were studied systematically.