• 文献标题:   Synthesis of clay-reduced graphene oxide composite catalysts for the electrochemical detection of flubendiamide: application in food samples
  • 文献类型:   Article
  • 作  者:   AGHRIS S, CHHAIBI B, ETTADILI FE, ALAOUI OT, LAGHRIB F, FARAHI A, BAKASSE M, LOUKILI A, LAHRICH S, EL MHAMMEDI MA
  • 作者关键词:   electroanalysi, food, insecticide, natural clay, exfoliated go
  • 出版物名称:   MATERIALS TODAY CHEMISTRY
  • ISSN:   2468-5194
  • 通讯作者地址:  
  • 被引频次:   0
  • DOI:   10.1016/j.mtchem.2022.101215 EA OCT 2022
  • 出版年:   2022

▎ 摘  要

This paper presents a simple and low-cost approach to synthesizing reduced graphene oxide/clay modified pencil electrode (rGO/Clay/PGE) through thermal reduction of GO/Clay for ultrasensitive detection of Flubendiamide (FBD). The graphene oxide (GO) was prepared by exfoliation of graphite with an eco-friendly procedure. The as-produced rGO/Clay was characterized by X-ray diffraction (XRD), Fourier transforms infrared spectroscopy (FT-IR), and Scanning electron microscopy (SEM). The elec-trochemical behavior of the synthesized electrode was studied by cyclic voltammetry (CV). Under optimized conditions, rGO/Clay/PGE exhibited excellent analytical properties toward FBD determination. A calibration curve was well-established from 0.1 to 100 mmol/L for FBD with a detection limit of 0.006 mmol/L. The method was successfully adopted for the detection of FBD in white rice samples.(c) 2022 Elsevier Ltd. All rights reserved.