▎ 摘　　要

In this article, novel molecularly imprinted polymers based on 3D reduced graphene oxide aerogel (3D RGO-GBMIPs) were successfully fabricated and applied as adsorbents for dispersed solid-phase extraction (DSPE) of ginkgolide B (GB). After being prepared by surface molecular imprinted technology, 3D RGO-GBMIPs were successively characterized by fourier transform infrared spectroscopy, thermogravimetric analysis, Raman spectroscopy, and scanning electron microscope. The results of adsorption experiments revealed that 3D RGO-GBMIPs presented highly selective recognition properties and well reusability. The main variables influencing DSPE efficiency, including extraction solvent, 3D RGO-GBMIPs dosage, category, and volume of eluent, as well as elution time were investigated. The DSPE results showed that 3D RGO-GBMIPs had an obvious effect on the improvement of GB purity in ginkgo biloba extract, with a satisfactory recovery rate and yield. Therefore, 3D RGO-GBMIPs are expected to be applied for the enrichment of GB from complex matrices.