• 文献标题:   Preparation of graphene by a low-temperature thermal reduction at atmosphere pressure
  • 文献类型:   Article
  • 作  者:   CHEN WF, YAN LF
  • 作者关键词:  
  • 出版物名称:   NANOSCALE
  • ISSN:   2040-3364 EI 2040-3372
  • 通讯作者地址:   Univ Sci Technol China
  • 被引频次:   246
  • DOI:   10.1039/b9nr00191c
  • 出版年:   2010

▎ 摘  要

It is still a challenge to prepare graphene from graphene oxide (GO) under a mild thermal reduction. Here we report that GO can even be reduced at a low temperature (below 150 degrees C) at atmospheric pressure in a mixture of N,N-dimethylacetamide (DMAc) and water (10 : 3, v/v) under the protection of nitrogen gas. FT-IR, XRD, XPS, Raman, and AFM studies confirmed the thermal reduction of GO and the formation of graphene. The as-prepared graphene can be fully dispersed in pure DMAc to form an organic suspension, and the suspension is stable for at least two months at room temperature.