▎ 摘　　要

Ag nanocubes-reduced graphene oxide(AgNCs-rGO) nanocomposite was successfully prepared by an in situ synthesis method, in which AgNCs were loaded onto the surface of rGO during the formation of AgNCs in an ethylene glycol solution. Characterization by X-ray diffraction, UV-Vis spectroscopy, and scanning electron micro-scopy indicated the successful preparation of the AgNCs-rGO nanocomposite. Most importantly, the AgNCs-rGO nanocomposite exhibited excellent electrocatalytic activity for the reduction of H2O2, leading to a high-performance non-enzymatic H2O2 sensor with a linear detection range and detection limit of approximately 0.1 mmol/L to 70 mmol/L(r=0.999) and 0.58 mu mol/L, respectively. Our present work provides a new and highly efficient method for fabricating high-performance electrochemical sensors.