• 文献标题:   Indentation Size Effect on Ag Nanoparticle-Modified Graphene/Sn-Ag-Cu Solders
  • 文献类型:   Article
  • 作  者:   XU LY, ZHANG ST, JING HY, WANG LX, WEI J, KONG XC, HAN YD
  • 作者关键词:   indentation size effect, hardnes, creep stress exponent, hardening effect, solder alloy
  • 出版物名称:   JOURNAL OF ELECTRONIC MATERIALS
  • ISSN:   0361-5235 EI 1543-186X
  • 通讯作者地址:   Tianjin Univ
  • 被引频次:   1
  • DOI:   10.1007/s11664-017-5822-0
  • 出版年:   2018

▎ 摘  要

This paper presents the results for the indentation size effect (ISE) on the creep stress exponent and hardness of 0.03 wt.% Ag-modified graphene nanosheet Sn-Ag-Cu solder alloys, using constant loading/holding and multi-cycle (CMC) loading methods, respectively. At each maximum load, with increasing indentation depth, the creep exponent first decreased and then increased. At the same strain rate, the stress exponent also showed the same tendency, increasing as the indentation depth (peak load) increased and then decreased. The hardness was measured continuously with increasing indentation depth by the CMC loading method. The hardness did not exhibit a decrease as the indentation depth increased, which differs from the classical description of the ISE. After an initial decrease, the hardness then increased and finally decreased as the indentation depth increased. This study reviews the existing theories and formulations describing ISE with hardening effects. The experimental results fit well with the empirical formulation. The phenomenon of ISE accompanied by hardening effects has been explained physically via the interaction between geometrically necessary dislocations and grain boundaries.