• 文献标题:   High yield and high concentration few-layer graphene sheets using solvent exfoliation of graphite with pre-thermal treatment in a sealed bath
  • 文献类型:   Article
  • 作  者:   HOSSAIN MM, PARK OK, HAHN JR, KU BC
  • 作者关键词:   carbon material, high dispersion, thermal activation, mechanical exfoliation, raman, graphene sheet
  • 出版物名称:   MATERIALS LETTERS
  • ISSN:   0167-577X EI 1873-4979
  • 通讯作者地址:   Chonbuk Natl Univ
  • 被引频次:   11
  • DOI:   10.1016/j.matlet.2014.03.024
  • 出版年:   2014

▎ 摘  要

We developed an efficient method for exfoliating pristine graphite in an organic solvent to produce a high yield (14%) and high concentration (5.25 mg/mL) of well-dispersed mono-, bi-, and multi-layered graphene sheets. Pre-thermal activation of pristine graphite at 900 degrees C in a sealed stainless steel bath under high pressure, followed by sonication in a solvent of 1-methyl-2-pyrrolidinone at elevated temperatures produced a solution of homogeneous, well-dispersed, defect-free, and non-oxidized graphene. The resulting electrical conductivities of the graphene sheets were high, up to 849 S/cm. (c) 2014 Elsevier B.V. All rights reserved.