• 文献标题:   Preparation, characterization and electrochemical performance of graphene from microcrystalline graphite
  • 文献类型:   Article
  • 作  者:   FANG CY, ZHANG Z, BING X, LEI Y
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF MATERIALS SCIENCEMATERIALS IN ELECTRONICS
  • ISSN:   0957-4522 EI 1573-482X
  • 通讯作者地址:   Wuhan Univ Technol
  • 被引频次:   1
  • DOI:   10.1007/s10854-017-7876-4
  • 出版年:   2017

▎ 摘  要

Microcrystalline graphite, a kind of economic and resourceful graphite material, was used to synthesize graphene by oxidation-reduction method. The graphite/KMnO4 ratios were adjusted in an oxidation process, and the produced graphite oxide and reduced graphene oxide were characterized by X-ray diffraction, transmission electron microscopy, ultraviolet-visible absorption spectroscopy and Fourier transform infrared spectroscopy. The electrochemical properties were evaluated by cyclic voltammetry in a three-electrode system. The curves maintain an ideal rectangular and symmetric shape, indicating that the product has good electrochemical properties. The results show that a remarkable increase in both the current density and specific capacitance can be observed for graphene at a graphite/KMnO4 ratio of 1:3.