• 文献标题:   Role of synthesis method on microstructure and mechanical properties of graphene/carbon nanotube toughened Al2O3 nanocomposites
  • 文献类型:   Article
  • 作  者:   YAZDANI B, PORWAL H, XIA YD, YAN HX, REECE MJ, ZHU YQ
  • 作者关键词:   al2o3, graphene nanoplatelet, carbon nanotube, hotpres, spark plasma sintering
  • 出版物名称:   CERAMICS INTERNATIONAL
  • ISSN:   0272-8842 EI 1873-3956
  • 通讯作者地址:   Univ Exeter
  • 被引频次:   10
  • DOI:   10.1016/j.ceramint.2015.04.054
  • 出版年:   2015

▎ 摘  要

The effects of hot-pressing (HP) and spark plasma sintering (SPS) methods on the grain size, microstructural features, and mechanical behaviour of graphene nanoplatelet/carbon nanotubes (GNTs) reinforced Al2O3 nanocomposites were comprehensively studied. Different graphene nanoplatelet to carbon nanotube ratios were selected as the overall reinforcement content of composites prepared using HP and SPS. Highly densified samples (> 98%) were obtained at 1650 degrees C under 40 MPa in Ar atmosphere, with dwell times of 1 h and 10 min for HP and SPS respectively. Both types of sample showed a mixture of inter- and transgranular fracture behaviour. A 50% grain size reduction was observed for samples prepared by HP compared to SPS samples. Both types of samples achieved a high flexural strength and fracture toughness of > 400 MPa and 5.5 MPa m(1/2), whilst SPS samples peaked at relatively lower GNT contents than those for the HP samples. Based on analyses of the morphology, grain sizes and fracture mode, similar toughening mechanisms for both types of sample were observed, involving the complex characteristics of the combined GNT fillers. (C) 2015 Elsevier Ltd and Techna Group S.r.l. All rights reserved.