• 文献标题:   One-pot synthesis of reduced graphene oxide nanosheets anchored ZnO nanoparticles via microwave approach for electrochemical performance as supercapacitor electrode
  • 文献类型:   Article
  • 作  者:   KUMAR R, YOUSSRY SM, ABDELGALEIL MM, MATSUDA A
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF MATERIALS SCIENCEMATERIALS IN ELECTRONICS
  • ISSN:   0957-4522 EI 1573-482X
  • 通讯作者地址:   Toyohashi Univ Technol
  • 被引频次:   0
  • DOI:   10.1007/s10854-020-04108-w EA AUG 2020
  • 出版年:   2020

▎ 摘  要

In this article, we have demonstrated single-step as well as scalable synthesis of zinc oxide nanoparticles (ZnO NPs) supported on highly thin/transparent reduced graphene oxide (rGO) nanocomposite (ZnO@rGO) via direct microwave irradiation using decomposition of zinc acetate dihydrate (Zn(CH3CO2)(2)center dot 2H(2)O) along with reduction of graphite oxide. The surface microstructure of prepared ZnO@rGO nanocomposite was analyzed by X-ray diffraction, transmission electron microscopy, scanning electron microscopy, Raman spectroscopy, and X-ray photo electron spectroscopy. Different characterization analysis indicates that the ZnO NPs in the nanocomposite were dispersed on the surfaces of rGO nanosheets (NSs). Raman spectra reveal the structural defects level of rGO NSs was 0.78, while it was increased to 1.66 for ZnO@rGO nanocomposites. The synthesized ZnO@rGO nanocomposite exhibits specific capacitance of 102.4 F/g at the scan rate of 30 mV/s and shows good cyclic stability of 82.5% for 3000 cycles at high scan rate 100 mV/s.