• 文献标题:   Synthesis and characterization of stable aqueous dispersions of graphene
  • 文献类型:   Article
  • 作  者:   SUR UK, SAHA A, DATTA A, ANKAMWAR B, SURTI F, ROY SD, ROY D
  • 作者关键词:   graphene, zeta potential, graphene oxide, graphite, dispersion, raman spectroscopy
  • 出版物名称:   BULLETIN OF MATERIALS SCIENCE
  • ISSN:   0250-4707 EI 0973-7669
  • 通讯作者地址:   Univ Calcutta
  • 被引频次:   15
  • DOI:   10.1007/s12034-015-0893-0
  • 出版年:   2016

▎ 摘  要

A stable aqueous dispersion (5 mg ml(-1)) of graphene was synthesized by a simple protocol based on three-step reduction of graphene oxide (GO) dispersion synthesized using the modified version of Hummers and Offeman method. Reduction of GO was carried out using sodium borohydride, hydrazine hydrate and dimethyl hydrazine as reducing agents. The chemically synthesized graphene was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV-visible absorption spectroscopy, Fourier transform infrared (FTIR) and Raman spectroscopy, thermogravimetric analysis (TGA), optical microscopy. The stability of aqueous dispersions of graphene was confirmed through zeta potential measurements and the negative zeta potentials of 55-60 mV were obtained indicating the high stability of aqueous graphene dispersions.