• 文献标题:   Preparation, Characterization and First Application of Graphene Oxide-Metformin-Nickel for the Suzuki Cross-Coupling Reaction
  • 文献类型:   Article
  • 作  者:   RAOUFI F, MONAJJEMI M, AGHAEI H, ZARE K, GHAEDI M
  • 作者关键词:   crosscoupling reaction, graphene oxide, nickel, suzukimiyaura reaction
  • 出版物名称:   CHEMISTRYSELECT
  • ISSN:   2365-6549
  • 通讯作者地址:   Islamic Azad Univ
  • 被引频次:   2
  • DOI:   10.1002/slct.201903749
  • 出版年:   2020

▎ 摘  要

In this project, in the first step, the graphene oxide-metformin-nickel catalyst has been prepared and then the Ni(II) was reduced to Ni(0) by hydrazine hydrate and Ni(0) nanoparticle coordinated to metformin-GO was achieved. After full characterization of catalyst structure by different analyses like fourier-transform infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-Ray analysis (EDX), X-Ray diffraction analysis (XRD), thermal gravimetric analysis (TGA), and coupled plasma/atomic emission spectroscopy (ICP), as well as confirm the successful synthesis of catalyst, the activity of catalyst has been examined in the Suzuki-Miyaura cross-coupling reaction.