• 文献标题:   A Green Approach to the Synthesis of Reduced Graphene Oxide using Sodium Humate
  • 文献类型:   Article
  • 作  者:   XIANG N, HUANG JG, ZHAO HG, LIU CJ, LIU XJ
  • 作者关键词:   graphene, graphene oxide, natural reducing agent, sodium humate
  • 出版物名称:   ZEITSCHRIFT FUR PHYSIKALISCHE CHEMIEINTERNATIONAL JOURNAL OF RESEARCH IN PHYSICAL CHEMISTRY CHEMICAL PHYSICS
  • ISSN:   0942-9352
  • 通讯作者地址:   Jilin Univ
  • 被引频次:   6
  • DOI:   10.1515/zpch-2016-0762
  • 出版年:   2016

▎ 摘  要

A green and simple chemistry approach was demonstrated to prepare reduced graphene oxide (rGO) using sodium humate (SH) as the reducing agent. Without using toxic and harmful chemicals, this method is environmentally friendly and suitable for the large-scale production of graphene. At first, the improved Hummers method to oxidize graphite for the synthesis of graphene oxide (GO) was applied, and then the as-prepared GO was reduced by SH to form rGO. Characterization was performed using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microscope (SEM), energy dispersive X-ray spectroscopy (EDX), X-ray photoelectron spectrometry (XPS) and Raman spectra. The intensity ratio of the D and G band (I D /I G) of GO after reduction with SH increases from 0.96 (GO) to 1.11 (rGO), the results obtained from the Raman spectra proved high purity of the final products.