• 文献标题:   Fabrication of oxide-free graphene suspension and transparent thin films using amide solvent and thermal treatment
  • 文献类型:   Article
  • 作  者:   OH SY, KIM SH, CHI YS, KANG TJ
  • 作者关键词:   graphene sheet, amide solvent, thermal treatment, transparent conductive film
  • 出版物名称:   APPLIED SURFACE SCIENCE
  • ISSN:   0169-4332 EI 1873-5584
  • 通讯作者地址:   Seoul Natl Univ
  • 被引频次:   16
  • DOI:   10.1016/j.apsusc.2012.05.101
  • 出版年:   2012

▎ 摘  要

High quality graphene sheets were produced from graphite by liquid phase exfoliation using N-methyl-2-pyrrolidone (NMP) and a subsequent thermal treatment to enhance the exfoliation. The exfoliation was enhanced by treatment with organic solvent and high thermal expansion producing high yields of the high-quality and defect-free graphene sheets. The graphene was successfully deposited on a flexible and transparent polymer film using the vacuum filtration method. SEM images of thin films of graphene treated at 800 degrees C showed uniform structure with no defects commonly found in films made of graphene produced by other techniques. Thin films of graphene prepared at higher temperatures showed superior transmittance and conductivity. The sheet-resistance of the graphene film treated at 800 degrees C was 2.8 x 10(3) k Omega/square with 80% transmittance. (C) 2012 Elsevier B. V. All rights reserved.