• 文献标题:   Preparation of Graphene Liquid Cells for the Observation of Lithium-ion Battery Material
  • 文献类型:   Article
  • 作  者:   CHANG JH, CHEONG JY, SEO HK, KIM ID, YUK JM
  • 作者关键词:   engineering, issue 144, graphene liquid cell, lithiumion battery, in situ transmission electron microscopy tem, electrode, electrolyte, electron beam
  • 出版物名称:   JOVEJOURNAL OF VISUALIZED EXPERIMENTS
  • ISSN:   1940-087X
  • 通讯作者地址:   Korea Adv Inst Sci Technol
  • 被引频次:   1
  • DOI:   10.3791/58676
  • 出版年:   2019

▎ 摘  要

In this work, we introduce the preparation of graphene liquid cells (GLCs), encapsulating both electrode materials and organic liquid electrolytes between two graphene sheets, and the facile synthesis of one-dimensional nanostructures using electrospinning. The GLC enables in situ transmission electron microscopy (TEM) for the lithiation dynamics of electrode materials. The in situ GLC-TEM using an electron beam for both imaging and lithiation can utilize not only realistic battery electrolytes, but also the high-resolution imaging of various morphological, phase, and interfacial transitions.