• 文献标题:   Preparation of Nitrogen-Doped Graphene with Solid Microwave Method
  • 文献类型:   Article
  • 作  者:   WANG K, JI BC, HAN MJ, LI LW
  • 作者关键词:   graphene, nitrogendoped, solid microwave
  • 出版物名称:   CHINESE JOURNAL OF INORGANIC CHEMISTRY
  • ISSN:   1001-4861
  • 通讯作者地址:   Qingdao Univ
  • 被引频次:   6
  • DOI:   10.3969/j.issn.1001-4861.2013.00.328
  • 出版年:   2013

▎ 摘  要

Graphite oxide was synthesized via Hummers method with flake graphite as raw material. After centrifugation and washing to clean out the remnant slat, ethylenediamine (EDA) was added into the dispersion to react with graphene oxides giving rise to functional graphene sheets (FGS). The dried FGS can interact with microwaves strongly, producing superheating which results in decomposing the grafted EDA molecules and in-situ doping graphene sheets. The morphology, structure, and components of the as-produced graphene were characterized by scanning electron microscopy (SEM), transmission electron microscope (TEM), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), energy dispersion spectrum (EDS). The results showed that nitrogen-doped graphene sheets (NGS) can be successfully synthesized via this strategy. The synthesized nitrogen-doped graphene was transparent.