• 文献标题:   Mechanically isotropic alumina prepared by spark plasma sintering: The role of pyrolytic carbon and multilayer graphene
  • 文献类型:   Article
  • 作  者:   FAN XH, NI N, WANG X, HAO W, GUO FW, ZHAO XF
  • 作者关键词:   alumina, multilayer graphene, pyrolytic carbon, fracture toughnes, anisotropy
  • 出版物名称:   JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
  • ISSN:   0955-2219 EI 1873-619X
  • 通讯作者地址:  
  • 被引频次:   2
  • DOI:   10.1016/j.jeurceramsoc.2021.01.056 EA MAR 2021
  • 出版年:   2021

▎ 摘  要

Anisotropy in mechanical properties is commonly reported in ceramics prepared by Spark Plasma Sintering (SPS). Here we investigate SPS preparation of isotropic alumina by adding pyrolytic carbon with and without multilayer graphene as sintering additives. Anisotropy in grain morphology, elastic modulus, microhardness and fracture toughness (KIC) is evaluated by a comparison of measurements along directions parallel and perpendicular to the external electric field in SPS. Results show that anisotropy in the first three parameters is insignificant except KIC. {0001} fiber texture attributes to anisotropy in pure alumina. As pyrolytic carbon adds, equiaxed grains in alumina are significantly refined mainly due to pinning effect and KIC increases because of induced microcracking. Anisotropy in KIC of the composite is reduced due to scattering of the {0001} fiber texture. When multilayer graphene with in-plane size in micron is further introduced, anisotropy in KIC is diminished at the cost of embrittlement.