• 文献标题:   Easy Preparation of Nanosilver-Decorated Graphene Using Silver Carbamate by Microwave Irradiation and Their Properties
  • 文献类型:   Article
  • 作  者:   YUN SW, CHA JR, GONG MS
  • 作者关键词:   silver nanoparticle, 1amino4methylpiperazine, silver alkylcarbamate, microwave, graphene/agnps composite
  • 出版物名称:   BULLETIN OF THE KOREAN CHEMICAL SOCIETY
  • ISSN:   0253-2964 EI 1229-5949
  • 通讯作者地址:   Dankook Univ
  • 被引频次:   7
  • DOI:   10.5012/bkcs.2014.35.8.2251
  • 出版年:   2014

▎ 摘  要

We have successfully decorated reduced graphene oxide (RGO) with silver nanoparticles (AgNPs) by microwaving silver alkylcarbamate for 13 seconds using 1-amino-4-methylpiperazine. Uniform AgNPs (20-40 nm) were effectively prepared, and 1-amino-4-methylpiperazine acted as a reaction medium, reducing agent, and stabilizer. Particle size and morphology were correlated with the silver alkylcarbamate concentration and microwave time. The graphene/AgNPs composites were characterized by Raman, X-ray diffraction, and scanning electron microscopy to confirm that the AgNPs were uniformly decorated onto the graphene. Measurements of the transparent conductive property at room temperature indicated that these graphene/AgNPs nanosheets with 55.45% transmittance were electrically continuous with a sheet resistance of approximately 43 k Omega/square.