• 文献标题:   Investigation of Structural and Thermal Properties of Graphene Oxide Reinforced Epoxy Nanocomposites
  • 文献类型:   Article
  • 作  者:   GAUR MS, RAGHAV RK, SAGAR R, TIWARI RK
  • 作者关键词:  
  • 出版物名称:   ECS JOURNAL OF SOLID STATE SCIENCE TECHNOLOGY
  • ISSN:   2162-8769 EI 2162-8777
  • 通讯作者地址:  
  • 被引频次:   0
  • DOI:   10.1149/2162-8777/ac5eb0
  • 出版年:   2022

▎ 摘  要

The nanocomposites thin film was prepared by adding exfoliated GO in epoxy-hardner solution in different weight ratio. We investigate the thermal and surface properties of epoxy-graphene oxide (GO) nanocomposites using differential scanning calorimetry (DSC), fourier transform infrared spectroscopy (FTIR), atomic force microscopy (AFM) and contact angle measurement method. AFM and contact angle results are supporting that graphene oxide provides the best reinforcement in epoxy. AFM is investigated the dispersion of GO and structural morphology of epoxy nanocomposites. The FTIR results show that exfoliated GO of two-dimensional (2D) shape favors the hardening process of the epoxy matrix, increasing its reaction rate by observing an epoxy stretching frequency at 907 cm(-1). The GO modified with amino group of epoxy lead to the increase of crosslinking density. FTIR absorption peak in 1700-1500 cm(-1) regions is due to amino group. This attributes the significant increase of glass transition temperature of epoxy/GO nanocomposites . The contact angle and surface roughness increases with increase in concentration of GO in epoxy shows roughness induced hydrophobic surface. The solid surface energy was calculated by contact angle favors the good dispersion of GO in epoxy matrix. (C) 2022 The Electrochemical Society ("ECS"). Published on behalf of ECS by IOP Publishing Limited.