• 文献标题:   Preparation and properties of nanocrystalline Ni/graphene composite coatings deposited by electrochemical method
  • 文献类型:   Article
  • 作  者:   CIESLAK G, TRZASKA M
  • 作者关键词:   graphene, electrodeposition, composite coating, ni/graphene coating
  • 出版物名称:   POLISH JOURNAL OF CHEMICAL TECHNOLOGY
  • ISSN:   1509-8117 EI 1899-4741
  • 通讯作者地址:   Inst Precis Mech
  • 被引频次:   1
  • DOI:   10.2478/pjct-2018-0005
  • 出版年:   2018

▎ 摘  要

The paper presents results of studies of composite nickel/graphene coatings produced by electrodeposition method on a steel substrate. The method of producing composite coatings with nanocrystalline nickel matrix and dispersion phase in the form of graphene is presented. For comparative purposes, the study also includes nano-crystalline Ni coatings produced by electrochemical reduction without built-in graphene flakes. Graphene was characterized by Raman spectroscopy, transmission and scanning electron microscopes. Results of studies on the structure and morphology of Ni and Ni/graphene layers produced in a bath containing different amounts of graphene are presented. Material of the coatings was characterized by SEM, light microscopy, X-ray diffraction. The microhardness of the coatings was examined by Knoop measurements. The adhesion of the coatings with the substrate was tested using a scratchtester. The influence of graphene on the structure and properties of composite coatings deposited from a bath with different graphene contents was determined.