• 文献标题:   Investigation of nickel slag waste as a modifier on graphene-TiO2 microstructure for sensing phenolic compound
  • 文献类型:   Article
  • 作  者:   WIBOWO D, SUFANDY Y, IRWAN I, AZIS T, MAULIDIYAH M, NURDIN M
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF MATERIALS SCIENCEMATERIALS IN ELECTRONICS
  • ISSN:   0957-4522 EI 1573-482X
  • 通讯作者地址:   Inst Teknol Dan Kesehatan Avicenna
  • 被引频次:   0
  • DOI:   10.1007/s10854-020-03996-2 EA JUL 2020
  • 出版年:   2020

▎ 摘  要

In the present work, the potential of nickel slag waste (NSW) was performed as a modifier of graphene-TiO2 material for sensing phenolic compound under an electrochemical system. It was provided to produce variations of mineral components to improve electrochemical sensing in its application for a sensor device. Preparation of composite material (slag-graphene-TiO2) was prepared through solid-state reaction by mixing of NSW, graphene, and TiO2 anatase crystal. Based on these results, we discover the composition of NSW with various mineral contents and produced anatase TiO2 crystal prepared via thermal method at 500 degrees C for 3 h. Subsequently, the slag-G-TiO2 composite has been homogeneous and characterized using SEM-EDX shows the microstructure formed with the variation of elements content. Moreover, the electrochemical test for sensing phenol compound exhibits the exceptionally sensitivity towards phenol detection in electrolyte solution by the limit of detection (LoD) is 0.0367 ppm and % RSD value of 0.016%. The electrode also produce excellent stability properties by repeatability of 1 to 21 times and the average of oxidation current at 183.57 mu A. Finally, we test with a real sample to obtain the ability of phenol detection.