• 文献标题:   Reassessing the Necessity of the Drying Step in Hummer's Method for Graphene Oxide Synthesis
  • 文献类型:   Article
  • 作  者:   GLASS DE, GALVAN V, PRAKASH GKS
  • 作者关键词:   graphene oxide, suspension, hummer s method, platinum, electrochemical reduction, capacitor
  • 出版物名称:   ELECTROANALYSIS
  • ISSN:   1040-0397 EI 1521-4109
  • 通讯作者地址:  
  • 被引频次:   3
  • DOI:   10.1002/elan.202100188 EA AUG 2021
  • 出版年:   2021

▎ 摘  要

The necessity of drying the graphene oxide suspension (GOsus) using Hummer's Method to produce graphene oxide (GO) powder was studied. The undried GOsus was compared to the dried GO. The GO materials were used as Pt supports via NaBH4 reduction for O-2 reduction. XRD patterns showed similar d-spacing in both while the half-cell tests of the Pt/rGOsus and Pt/rGO catalysts were similar. GOsus film, deposited onto Toray Carbon Paper and electrochemically reduced in aq. H2SO4 was tested as a capacitor. The suspension and dried graphene-based capacitor showed similar XRD and XPS patterns and the erGOsus capacitor displayed increased capacitance.