• 文献标题:   Facile sonochemical synthesis of perovskite-type SrTiO3 nanocubes with reduced graphene oxide nanocatalyst for an enhanced electrochemical detection of alpha-amino acid (tryptophan)
  • 文献类型:   Article
  • 作  者:   GOVINDASAMY M, WANG SF, PAN WC, SUBRAMANIAN B, RAMALINGAM RJ, ALLOHEDAN H
  • 作者关键词:   sonochemical synthesi, perovskitetype srtio3, reduced graphene oxide, electrochemical sensor, amino acid detection
  • 出版物名称:   ULTRASONICS SONOCHEMISTRY
  • ISSN:   1350-4177 EI 1873-2828
  • 通讯作者地址:   Natl Taipei Univ Technol
  • 被引频次:   45
  • DOI:   10.1016/j.ultsonch.2019.04.004
  • 出版年:   2019

▎ 摘  要

In this paper, perovskite-type SrTiO3 nanocubes decorated reduced graphene oxide is synthesized by sonochemical method. The as-synthesized SrTiO3@RGO nanocomposite was confirmed by XRD, TEM, SEM, elemental mapping and electrochemical technique. Furthermore, surface morphological and X-ray diffraction studies revealed the formation and high loading of SrTiO3 nanocubes on reduced graphene oxide matrix. The SrTiO3@RGO nanocomposite modified electrode shows an excellent electrochemical detection towards of amino acid (tryptophan). The developed sensor was showed a wide linear range from 30 nM to 917.3 mu M and detection limit is 7.15 nM. Furthermore, the sensitivity was calculated to be 9.11 mu A mu M-1 cm(2). In addition, the proposed modified sensor is exhibited good selectivity, stability, reproducibility and repeatability. The SrTiO3@RGO catalyst modified electrode was successfully applied to tryptophan analysis in biological samples.