▎ 摘　　要

Graphene oxide (GO) have been synthesized and doped with nickel metal salt under differ thermal conditions. The doped graphene oxides obtained were characterized by Fourier transform infrared spectroscopy (FTIR), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Raman spectroscopy, and Atomic force spectroscopy AFM). The results obtained indicate difference between the crystallinity pattern of microwave and the conventional heating system of the materials and the progressive formation of transparent and decorated graphene with nickel particles which increases with temperature.