• 文献标题:   Micro-mechanical properties and multi-scaled pore structure of graphene oxide cement paste: Synergistic application of nanoindentation, X-ray computed tomography, and SEM-EDS analysis
  • 文献类型:   Article
  • 作  者:   LONG WJ, GU YC, XIAO BX, ZHANG QM, XING F
  • 作者关键词:   graphene oxide, microstructure, nanoindentation, micromechanical propertie, xray computed tomography, pore
  • 出版物名称:   CONSTRUCTION BUILDING MATERIALS
  • ISSN:   0950-0618 EI 1879-0526
  • 通讯作者地址:   Shenzhen Univ
  • 被引频次:   4
  • DOI:   10.1016/j.conbuildmat.2018.05.229
  • 出版年:   2018

▎ 摘  要

In this study, the microstructure and micromechanical properties of graphene oxide (GO) cement-based materials are investigated. Nanoindentation with statistical deconvolution was used to determine the elastic properties of constituent phases. Besides, combined with scanning electron microscopy (SEM) equipped with energy-dispersive spectrometer (EDS) and backscattered electrons (BSE), each phase of hardened cement paste was identified and quantified as well. X-ray computed tomography (XCT) microscope was applied to determine the morphology of micrometer-size pores, while mercury intrusion porosimetry (MIP) was used to capture the volume fraction of smaller pores (nano-scale). The combined use of XCT and MIP offered an effective approach for further understanding the effect of GO on pore structure at multi-scale. The synergistic analysis of microstructure and micromechanical properties at multi-scale provides valuable information towards the material design of cement-based materials with nanomaterials. (C) 2018 Elsevier Ltd. All rights reserved.