• 文献标题:   Preparation of nickel-graphene composites by jet electrodeposition and the influence of graphene oxide concentration on the morphologies and properties
  • 文献类型:   Article
  • 作  者:   JI LL, CHEN FD, HUANG H, SUN XY, YAN YY, TANG XB
  • 作者关键词:   nickelgraphene composite, jet electrodeposition, graphene oxide, microhardnes, electrochemical corrosion propertie
  • 出版物名称:   SURFACE COATINGS TECHNOLOGY
  • ISSN:   0257-8972
  • 通讯作者地址:   Nanjing Univ Aeronaut Astronaut
  • 被引频次:   2
  • DOI:   10.1016/j.surfcoat.2018.07.083
  • 出版年:   2018

▎ 摘  要

Nickel-graphene (N-G) composites are potential candidate structural materials for molten salt reactors. A rapid preparation method for these composites by jet electrodeposition was developed, and the microstructure, microhardness, and corrosion properties of these composites were studied to explore the key parameters of the jet electrodeposition. Results indicated that the distribution of graphene in composites mainly depended on the concentration of graphene oxide (GO) in the plating solution. Composites deposited with GO concentration of 0, 0.5, 1 g/L showed surface root-mean-square roughness value (Rq) of 6, 12, and 28 nm, respectively. Meanwhile with the increase of GO concentration, the Hardness value became larger. The corrosion potential E-corr and current I-corr of composites obtained at 0.5 g/L with the best surface quality were 193 mV and 5.7 x 10(-6) A/cm(2), respectively, which indicated the best electrochemical corrosion resistance. Hydrogen annealing can help self-repair of graphene microstructure.