• 文献标题:   Preparation of Colloidal Dispersions of Graphene Sheets in Organic Solvents by Using Ball Milling
  • 文献类型:   Article
  • 作  者:   ZHAO WF, WU FE, WU H, CHEN GH
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF NANOMATERIALS
  • ISSN:   1687-4110 EI 1687-4129
  • 通讯作者地址:   Huaqiao Univ
  • 被引频次:   44
  • DOI:   10.1155/2010/528235
  • 出版年:   2010

▎ 摘  要

A top-down method was developed for producing colloidal dispersions of graphene sheets. Graphite nanosheets comprising hundreds of carbon layers were dispersed and gently ball-milled to exfoliate into graphene in a variety of organic solvents. After 30 hours of the shear-force-dominated grinding and a subsequent 4000 r.p.m. of centrifugation, single-and few-layer graphene sheets were readily prepared and homogeneously and stably suspended in the good solvent medium which possesses a surface tension value close to 40 mJ m(-2), such as in N,N-dimethylformamide, at a concentration up to 0.08 mg ml(-1), achieving a yield higher than 32.0 wt%. The graphene materials in the colloidal suspension were characterized using scanning and transmission electron microscopy and atomic force microscopy.