• 文献标题:   Experimental Multi-scale analysis of Carbon/Epoxy Composites Nano-Reinforced by Carbon Nanotubes/Multi-layer Graphene
  • 文献类型:   Article, Proceedings Paper
  • 作  者:   LEAO SG, MARTINS MGD, MENEZES NCF, LIMA FLRD, SILVA CF, ARANTES GC, AVILA AF
  • 作者关键词:   carbo fiber/epoxy laminate, graphene, carbon nanotube, failure mode, hybrid nanocomposite
  • 出版物名称:   MATERIALS RESEARCHIBEROAMERICAN JOURNAL OF MATERIALS
  • ISSN:   1516-1439 EI 1980-5373
  • 通讯作者地址:   Univ Fed Minas Gerais
  • 被引频次:   0
  • DOI:   10.1590/1980-5373-MR-2017-0976
  • 出版年:   2017

▎ 摘  要

Nano-size structures, nanotubes/multi-layer graphene (CNT/MLG), were dispersed into epoxy system by a combination of sonication and high shear mixing. To avoid CNT/MLG agglomeration, a non-covalent functionalization were performed using surfactants, CO890 - Polyoxyethylene (40) nonylphenyl ether and SDBS - sodium dodecyl benzene sulfonate. Raman spectroscopy and Fourier transformed Infra-red analysis indicated that CO890-MLG and SDBS-CNT have strong chemical interactions. Atomic force microscopy revealed formation of "spike-like" nanostructures for SDBS-CNT combination and "wall-like" nano-shape structures for the CO890-MLG ones. Tensile tests data indicate no significant change on stiffness. In average, the ultimate stress increased around 18%, while toughness had an improvement close to 62%. SDBS-CNT and CO890-MLG at small concentrations (0.075 wt. %) are probably the best options for nano-reinforcement of carbon/epoxy composites.