• 文献标题:   Understanding the Effects of Graphene Coating on the Electrostatic Field at the Tip of an Atom Probe Tomography Specimen
  • 文献类型:   Article
  • 作  者:   EXERTIER F, WANG JT, FU J, MARCEAU RKW
  • 作者关键词:   application to nonconductive biological specimen, atom probe tomography, chargestate ratio, fieldevaporation, graphene coating, voltagepulse apt
  • 出版物名称:   MICROSCOPY MICROANALYSIS
  • ISSN:   1431-9276 EI 1435-8115
  • 通讯作者地址:  
  • 被引频次:   2
  • DOI:   10.1017/S1431927621012356 EA JUL 2021
  • 出版年:   2022

▎ 摘  要

As a three-dimensional characterization method, atom probe tomography can provide key information that other methods cannot offer. Conductive coatings have proved to be an effective way for biological samples, and nonconductive samples in general, to be analyzed using voltage-pulsed atom probe tomography. In this study, we analyzed the effects of graphene coating on an electrically conductive material and were able to confirm the detection of carbon atoms. We compare quantitative electrostatic field metrics for a single-coated and a multi-coated specimen and measure both a reduced voltage after graphene coating and lowered charge-state ratios for different ion species, suggesting a lowered evaporation field related to the graphene coating. This information will be instructive for future studies on graphene-coated, nonconductive biological specimens.