• 文献标题:   Electrochemical synthesis and characterization of palladium nanoparticles on nafion-graphene support and its application for Suzuki coupling reaction
  • 文献类型:   Article
  • 作  者:   SHENDAGE SS, PATIL UB, NAGARKAR JM
  • 作者关键词:   electrochemical, palladium nanoparticle, nafiongraphene, heterogeneous catalyst
  • 出版物名称:   TETRAHEDRON LETTERS
  • ISSN:   0040-4039
  • 通讯作者地址:   Inst Chem Technol Deemed Univ
  • 被引频次:   40
  • DOI:   10.1016/j.tetlet.2013.04.092
  • 出版年:   2013

▎ 摘  要

The electrochemically deposited palladium nanoparticles on nafion-graphene support showed an excellent catalytic activity for Suzuki coupling reactions. The as obtained catalyst was characterized by SEM, TEM, EDAX, XRD, and TGA. The particle size of palladium nanoparticles (Pd NPs) determined from TEM was in the range of 4-12 nm. The mean diameter of Pd NPs was found to be 8.1 +/- 1.9 nm. The recyclability of the catalyst was examined and it did not show any significant loss of catalytic activity for five consecutive cycles. (C) 2013 Elsevier Ltd. All rights reserved.