• 文献标题:   Optimization of graphene nanoplatelets dispersion and nano-filler loading in bio-based polymer nanocomposites based on tensile and thermogravimetry analysis
  • 文献类型:   Article
  • 作  者:   SHAHDAN D, CHEN RS, AHMAD S
  • 作者关键词:   dispersion, distribution, graphene, mechanical propertie, thermal propertie, ultrasonic treatment
  • 出版物名称:   JOURNAL OF MATERIALS RESEARCH TECHNOLOGYJMR T
  • ISSN:   2238-7854 EI 2214-0697
  • 通讯作者地址:  
  • 被引频次:   5
  • DOI:   10.1016/j.jmrt.2021.08.130 EA SEP 2021
  • 出版年:   2021

▎ 摘  要

The incorporation of graphene nanoplatelets (GNPs) has attracted massive attention in polymer nanocomposite production. In this work, GNPs reinforced nanocomposites of liquid natural rubber (LNR) toughened poly (lactic acid) (PLA)/poly (aniline) (PANi) were fabricated through melt-mixing using internal mixer. The effects of ultrasonic treatment period, mixing rotor speed and GNPs loadings in PLA-LNR/PANi was investigated. A premix ultrasonication of LNR/PANi with GNPs for 1 h was found to be the most effective period as compared to the longer sonication time. The best melt-mixing of the materials was achieved at 100 rpm, in accordance to the tensile properties as well as homogeneous dispersion and distribution of nano-filler as shown in thermogravimetry analysis. Results revealed that the optimum loading was found at 0.4 wt.% of GNPs with excellent enhancement in tensile strength (25 MPa), tensile modulus (1188.9 MPa) and thermal stability of the nanocomposite, as proven by ANOVA statistical analysis. (c) 2021 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).