• 文献标题:   Evolution of photoelectron spectra at thermal reduction of graphene oxide
  • 文献类型:   Article
  • 作  者:   AFANAS EV VP, BOCHAROV GS, ELETSKII AV, RIDZEL OY, KAPLYA PS, KOPPEN M
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF VACUUM SCIENCE TECHNOLOGY B
  • ISSN:   2166-2746
  • 通讯作者地址:   Raspletina St 15
  • 被引频次:   3
  • DOI:   10.1116/1.4994788
  • 出版年:   2017

▎ 摘  要

The dynamics of graphene oxide (GO) reduction process is investigated by the electron spectroscopy. GO samples were obtained by the standard Hummers method with the subsequent thermal treatment at different temperatures. Photoelectron emission spectra (PES) of C 1s core level and its energy loss range are analyzed using the invariant imbedding principle. The differential single scattering inelastic cross sections x(in)(Delta) of all the GO samples were derived by using the fitting procedure. Simulation of PES is performed by making use of the partial intensity approach. The cross sections dynamics analysis shows the reduction process of the graphene structure with increasing annealing temperature. Thermal treatment at a temperature of 600 degrees C results in the appearance of p-plasmon peak. (C) 2017 American Vacuum Society.