• 文献标题:   (Ta,Nb)C composites formed with graphene nanoplatelets by spark plasma sintering
  • 文献类型:   Article, Proceedings Paper
  • 作  者:   RUDOLF CC, ERANEZHUTH B, BOESL B, AGARWAL A
  • 作者关键词:   fieldassisted sintering, microstructure control, dense ceramic, sintering additive, graphene, indentation
  • 出版物名称:   JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
  • ISSN:   0955-2219 EI 1873-619X
  • 通讯作者地址:   Florida Int Univ
  • 被引频次:   4
  • DOI:   10.1016/j.jeurceramsoc.2016.11.017
  • 出版年:   2017

▎ 摘  要

TaC-NbC with the addition of sintering additive (5 vol.% B4C or 5 vol.% Si) and 3 vol.% Graphene Nanoplatelets (GNP) are consolidated by spark plasma sintering (SPS). GNP are aligned in a uniformly oriented direction perpendicular to the processing axis of the SPS equipment during consolidation. High load instrumented indentation is performed and the projected area of residual damage is compared to estimate relative fracture toughness. The projected residual damaged area after indentation in the surface direction (out-of-plane GNP orientation) was 89% greater in the TaC-NbC-5B4C-3GNP sample, and 96% greater in the TaC-NbC-5Si-3GNP sample when compared to indentation in the orthogonal (in plane GNP orientation) direction. The toughening mechanisms prevalent in the orthogonal indentation direction (crack bridging and crack deflection) result in greater energy dissipation than the prevalent mechanisms in the surface indentation orientation (sheet sliding, crack bridging, and crack arrest). (C) 2016 Elsevier Ltd. All rights reserved.