• 文献标题:   Effect of Graphene Nanosheets Content on Microstructure and Mechanical Properties of Titanium Matrix Composite Produced by Cold Pressing and Sintering
  • 文献类型:   Article
  • 作  者:   HAGHIGHI M, SHAERI MH, SEDGHI A, DJAVANROODI F
  • 作者关键词:   titanium matrix composite, mechanical propertie, microstructure, graphene nanosheet
  • 出版物名称:   NANOMATERIALS
  • ISSN:   2079-4991
  • 通讯作者地址:   Imam Khomeini Int Univ
  • 被引频次:   3
  • DOI:   10.3390/nano8121024
  • 出版年:   2018

▎ 摘  要

The effect of graphene nanosheet (GNS) reinforcement on the microstructure and mechanical properties of the titanium matrix composite has been discussed. For this purpose, composites with various GNS contents were prepared by cold pressing and sintering at various time periods. Density calculation by Archimedes' principle revealed that Ti/GNSs composites with reasonable high density (more than 99.5% of theoretical density) were produced after sintering for 5 h. Microstructural analysis by X-ray diffraction (XRD) and a field emission scanning electron microscope (FESEM) showed that TiC particles were formed in the matrix during the sintering process as a result of a titanium reaction with carbon. Higher GNS content as well as sintering time resulted in an increase in TiC particle size and volume fraction. Microhardness and shear punch tests demonstrated considerable improvement of the specimens' mechanical properties with the increment of sintering time and GNS content up to 1 wt. %. The microhardness and shear strength of 1 wt. % GNS composites were enhanced from 316 HV and 610 MPa to 613 HV and 754 MPa, respectively, when composites sintered for 5 h. It is worth mentioning that the formation of the agglomerates of unreacted GNSs in 1.5 wt. % GNS composites resulted in a dramatic decrease in mechanical properties.