• 文献标题:   One-pot synthesis of chromenes in the presence of magnetic nanocomposite based on NH2 -UiO-66(Zr), graphene oxide and Fe3O4
  • 文献类型:   Article
  • 作  者:   ABDOLLAHIBASIR MH, SHIRINI F, TAJIK H, GHASEMZADEH MA
  • 作者关键词:   synthesis of chromene, magnetic nanocomposite, graphene oxide, uio66nh2, fe3o4
  • 出版物名称:   JOURNAL OF MOLECULAR STRUCTURE
  • ISSN:   0022-2860 EI 1872-8014
  • 通讯作者地址:  
  • 被引频次:   2
  • DOI:   10.1016/j.molstruc.2022.133022 EA APR 2022
  • 出版年:   2022

▎ 摘  要

In this research, GO/Fe3O4/UiO-66-NH2, a new magnetically recoverable heterogeneous catalyst, was prepared and characterized using various spectroscopic techniques and elemental analysis methods. The promoting ability of GO/Fe3O4/UiO-66-NH2 was studied in the synthesis of chromenes via one-pot three-component condensation of 4-hydroxycoumarin, 2-hydroxynaphthalene-1,4-dione and aromatic aldehydes at 110 degrees C under solvent-free conditions. This new protocol is included some important features such as lower loading of the catalyst, excellent yields (88%-98%), short reaction times (5-10 min), easy work-up procedure, and easy recovery using a simple magnet. The catalyst was characterized by SEM, XRD, EDX, BET, TGA and FT-IR analysis. (C) 2022 Elsevier B.V. All rights reserved.