• 文献标题:   Solvothermal Synthesis of Sb2S3-Graphene Oxide Nanocomposite for Electrochemical Detection of Dopamine
  • 文献类型:   Article
  • 作  者:   GAO L, MA JP, ZHENG JB
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF THE ELECTROCHEMICAL SOCIETY
  • ISSN:   0013-4651 EI 1945-7111
  • 通讯作者地址:   Northwest Univ
  • 被引频次:   0
  • DOI:   10.1149/1945-7111/ab82fc
  • 出版年:   2020

▎ 摘  要

Antimony sulfide graphene oxide (Sb2S3-GO) was synthesized using a solvothermal method for electrochemical detection of dopamine (DA). Thiourea acted as a sulfur source, while polyvinyl pyrrolidone (PVP) acted as a surfactant to fabricate nanoproduct in the presence of GO. X-ray diffraction spectroscopy (XRD), Fourier transform infrared spectroscopy (FTIR), Raman spectra, Energy-dispersive X-ray spectrum (EDS), Scanning electron microscopy (SEM) and Transmission electron microscopy (TEM) were employed to characterize Sb2S3-GO nanocomposite, and the results exhibited a large number of spherical Sb2S3 particles were attached to the surface of GO. Electrochemical techniques were used to study the performance of sensor, and the results showed the sensor has excellent electrochemical characteristics to detect DA with linear ranges of 1.55 mu M-15.55 mu M, 15.55 mu M-0.35 mM, excellent sensitivity of 307.7 mu A mM(-1) cm(-2) and 205.4 mu A mM(-1) cm(-2), and a low detection limit of 0.8 mu M (at an S/N radio of 3). Therefore, Sb2S3-GO can be used potential sensing material to detect dopamine. (C) 2020 The Electrochemical Society ("ECS"). Published on behalf of ECS by IOP Publishing Limited.