• 文献标题:   Preparation and Characterization of Graphene/Fe3O4 Composites by Solvothermal Method
  • 文献类型:   Article
  • 作  者:   ZHOU L, PENG XL, WANG XQ, JIN DF, JIN HX, GE HL
  • 作者关键词:   graphene/fe3o4 nanocomposite, sovolthernnal method, magnetic propertie, microstructure, morphologie
  • 出版物名称:   JOURNAL OF NANOSCIENCE NANOTECHNOLOGY
  • ISSN:   1533-4880 EI 1533-4899
  • 通讯作者地址:   China Jiliang Univ
  • 被引频次:   3
  • DOI:   10.1166/jnn.2015.9758
  • 出版年:   2015

▎ 摘  要

In the present study, graphene/Fe3O4 nanocomposites were prepared by solvothermal method using graphite oxide (GO) and FeCl3 center dot 6H(2)O as starting materials and the products were characterized by X-ray Diffraction (XRD), Scanning Electronic Microscope (SEM) and Vibrating Sample Magnetometer (VSM). Effects of Fe ion concentration, temperature and time of solvothermal reaction on the magnetic properties, microstructures and morphologies of graphene/Fe3O4 nanocomposites were investigated. The results showed that with the raising of Fe ion, particle size of the products became bigger, and saturation magnetization of the products got higher. The saturation magnetization and particle size of the products can be enhanced by increasing the reaction time and temperature, but the change of saturation magnetization and particle size were not obvious after the time got 8 h and temperature was at 200 degrees C, which demonstrated that the products became stable under this condition. The morphologies, microstructures and properties of products can be controlled by adjusting synthesis conditions.