▎ 摘　　要

Humic acids (HAs) isolated from high-moor peat have been studied by magic-angle spinning solid-state nuclear magnetic resonance (NMR) spectroscopy, differential scanning calorimetry (DSC), thermogravimetry (TG), and Raman spectroscopy. A composite of HAs with graphene oxide (GO) has been prepared for the first time, and the thermal carbonization (900 degrees C) of both HAs and the HA-GO composite has been carried out. With the use of mass spectrometry, it has been found that CO2 and H2O molecules are mainly released from HAs into the gas phase at a low temperature (to 150 degrees C). At higher temperatures, carbon monoxide and different low-molecular-weight hydrocarbons also begin to be released. From microscopic examinations, it follows that HA forms small agglomerates with sharply outlined edges as a result of carbonization, whereas the composite forms only large aggregates.