▎ 摘 要
In this study, graphene colloids were prepared using the electric spark discharge method (ESDM) with graphite rods (99.9% purity) in deionized water (DW) at a normal temperature and pressure. Five different types of graphene colloids were prepared using an electrical discharge machine (EDM) with five different pulse cycle switching times (T-on:T-off) = 10:10, 30:30, 50:50, 70:70, and 90:90 us. According to the Ultraviolet-visible spectra (UV-Vis) and Zetasizer analysis, the results showed that the 10:10 mu s parameter was the most suitable for the preparation of graphene colloids. UV-Vis was also used to detect the concentration of the graphene colloids; a comparison with a graphene oxide (GO) confirmed that this method could be used to calculate the discharge time needed to produce graphene colloids with different concentrations in the ESDM process.