• 文献标题:   Characterization of hydroxyapatite-reduced graphene oxide nanocomposites consolidated via high frequency induction heat sintering method
  • 文献类型:   Article, Early Access
  • 作  者:   NOSRATI H, SARRAFMAMOORY R, KAZEMI MH, PEREZ MC, SHOKROLLAHI M, EMAMEH RZ, FALAK R
  • 作者关键词:   hydroxyapatite, hydrothermal, graphene oxide, nanocomposite
  • 出版物名称:   JOURNAL OF ASIAN CERAMIC SOCIETIES
  • ISSN:   2187-0764
  • 通讯作者地址:   Tarbiat Modares Univ
  • 被引频次:   0
  • DOI:   10.1080/21870764.2020.1842119 EA NOV 2020
  • 出版年:  

▎ 摘  要

In this study, a solvothermal method at the temperature of 180 degrees C for 4 h was used for the synthesis of hydroxyapatite-reduced graphene oxide (HA-rGO) nanopowders by employing the nitrogen gas injection. To synthesize the powders, a solvent containing dimethylformamide, anhydrous ethanol, diethylene glycol, and water was used (1:1:1:2, respectively). Calcium nitrate tetrahydrate and diammonium hydrogenphosphate were used as calcium and phosphate precursors, respectively. The synthesized powders were consolidated by a high-frequency induction heat sintering method. The powders and sintered samples were then evaluated using X-ray diffraction, Raman spectroscopy, high-resolution transmission electron microscopy, Vickers indentation technique, and biocompatibility assay. The findings of this study showed that the final powders synthesized by the solvothermal method had calcium to phosphate ratio of about 1.67. The high frequency induction heat sintering method was suitable for consolidating these powders and exhibited a higher relative density than other methods. The mechanical properties of the nanocomposite were higher than those of pure HA. In biological experiments the difference of HA effect in comparison with the nanocomposite was not significant and both were biocompatible. [GRAPHICS]