• 文献标题:   Substrate free synthesis of graphene nanoflakes by atmospheric pressure chemical vapour deposition using Ni powder as a catalyst
  • 文献类型:   Article
  • 作  者:   SENGUPTA J, DAS K, NANDI UN, JACOB C
  • 作者关键词:   graphene nanoflake, chemical vapour deposition, xray diffraction, electron microscopy, raman spectroscopy
  • 出版物名称:   BULLETIN OF MATERIALS SCIENCE
  • ISSN:   0250-4707 EI 0973-7669
  • 通讯作者地址:   Jogesh Chandra Chaudhuri Coll
  • 被引频次:   0
  • DOI:   10.1007/s12034-019-1818-0
  • 出版年:   2019

▎ 摘  要

Graphene nanoflakes (GNFs) were synthesized by atmospheric pressure chemical vapour deposition of propane (C3H8) employing Ni (salen) powder without the introduction of a substrate. The graphitic nature of the GNFs was examined by an X-ray diffraction method. Scanning electron microscopy results revealed that GNFs were stacked on top of one another and had a high aspect ratio. Transmission electron microscopy studies suggested that the GNFs were made up of a number of crystalline graphene layers, some of which were even single crystalline as evident from the selected area diffraction pattern. Finally, Raman spectroscopy confirmed the high quality of the GNFs.