• 文献标题:   Scalable Preparation of Graphene: Effect of Synthesis Methods on the Material Characteristics
  • 文献类型:   Article
  • 作  者:   VAN NANG L, HOA ND, VAN PHUOC C, QUY CT, VAN TONG P, VAN QUANG V, VAN DUY N, VAN HIEU N
  • 作者关键词:   graphene, graphene oxide, wetchemical method, gas sensor
  • 出版物名称:   SCIENCE OF ADVANCED MATERIALS
  • ISSN:   1947-2935 EI 1947-2943
  • 通讯作者地址:   Hanoi Univ Sci Technol
  • 被引频次:   9
  • DOI:   10.1166/sam.2015.2171
  • 出版年:   2015

▎ 摘  要

Synthesis of graphene with scalable characteristics, quality, and quantity has drawn much attention because of its massive potential application. Herein, we introduce a facile and scalable synthesis of graphene by direct-reduction and hydrothermal methods. The direct-reduction method involved the reduction of graphene oxide using ascorbic acid at 60 degrees C, whereas the hydrothermal method was performed using the same precursor under high pressure and at 160 degrees C. The effects of the synthesis pathways on the graphene characteristics and quality were investigated through Raman spectroscopy, scanning electron microscopy, transmission electron microscopy, and gas sensing measurements. Results demonstrated that the hydrothermal method was effective for the fabrication of graphene with scalable quantity. Gas-sensing characteristics of the high-quality synthesized graphene were tested against NO2 and Cl-2 gases at different temperatures. The results demonstrated that the graphene sensors could detect the toxic oxidizing gases investigated with reasonable response and good response/ recovery characteristics, suggesting a great potential application in air pollution monitoring.