• 文献标题:   Contact-mechanical properties at pre-creep temperatures of fine-grained graphene/SiC composites prepared in situ by spark-plasma sintering
  • 文献类型:   Article
  • 作  者:   ROMANMANSO B, SANCHEZGONZALEZ E, ORTIZ AL, BELMONTE M, OSENDI MI, MIRANZO P
  • 作者关键词:   sic, graphene, composite, contactmechanical propertie, sparkplasma sintering, hertzian indentation test
  • 出版物名称:   JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
  • ISSN:   0955-2219 EI 1873-619X
  • 通讯作者地址:   Univ Extremadura
  • 被引频次:   18
  • DOI:   10.1016/j.jeurceramsoc.2013.11.003
  • 出版年:   2014

▎ 摘  要

Hertzian indentation was used to investigate for the first time the elastic plastic behavior and contact damage evolution with temperature (in the 25-850 degrees C range) in air of different in situ grown graphene/SiC composites. Three SiC starting powders differing in polytypes and particle sizes were liquid-phase densified by spark-plasma sintering, thus producing ceramic composites that contain about 4 vol.% of epitaxial grown graphene flakes at the grain boundaries and have interesting differences in their microstructure. The general trend in the contact mechanical behavior is qualitatively similar among the different composites, with the elastic modulus, yield stress, and critical loads for the onset of quasi-plasticity and ring/cone cracking all decreasing with increasing temperature, with the differences at the quantitative level being explained in terms of the particular microstructure of each graphene/SiC composite. (C) 2013 Elsevier Ltd. All rights reserved.