▎ 摘 要
In this article, samples of phenolic resin reinforced with graphene oxide were prepared. Mechanical properties of the composite were tested. Dynamic mechanical analysis, Fourier transform infrared spectroscopy, Differential scanning calorimetry, and thermogravimetric analysis were employed to study the mechanical properties in varied temperatures to infer the influence of graphene oxide on thermal performance of phenolic resin. The results show that the addition of graphene oxide resulted in a significant improvement in the elastic modulus of phenolic resin; Young's modulus, and tensile strength increase along with the graphene oxide content. Esterification reaction happened between alcohol OH groups on resole and carbonyl (sbond]COOH) groups on graphene oxide. Addition of graphene oxide improved residue rate of phenolic resin by 5.8%, whereas the temperature distribution of phenolic pyrolysis stay unchanged. The glass transition temperature of phenolic resin has been improved by 30 degrees C. POLYM. COMPOS. 34:1245-1249, 2013. (c) 2013 Society of Plastics Engineers