• 文献标题:   A time efficient reduction strategy for bulk production of reduced graphene oxide using selenium powder as a reducing agent
  • 文献类型:   Article
  • 作  者:   TIWARI SK, HUCZKO A, ORAON R, DE ADHIKARI A, NAYAK GC
  • 作者关键词:  
  • 出版物名称:   JOURNAL OF MATERIALS SCIENCE
  • ISSN:   0022-2461 EI 1573-4803
  • 通讯作者地址:   Indian Sch Mines
  • 被引频次:   12
  • DOI:   10.1007/s10853-016-9903-x
  • 出版年:   2016

▎ 摘  要

This work reports a time effective and facile reduction of graphene oxide to few-layered reduced graphene oxide (rGO) using a very minute amount of selenium powder at 360 A degrees C in a sealed tube. The prepared samples were purified and analyzed with field emission scanning electron microscopy, atomic force microscopy, Fourier transform infrared spectroscopy, X-ray diffraction, X-ray photoelectron spectroscopy, ultraviolet-visible spectroscopy, and Raman spectroscopy which confirmed the formation of few-layered rGO. It seems that high surface area (795 m(2) g(-1)) of prepared bulk rGO by this path would be a better option for polymer chemist to develop cheaper and highly reinforced rGO-based blend materials for the various thermo-mechanical applications.