• 文献标题:   Synthesis of Nitrogen Doped Multilayered Graphene Flakes: Selective Non-enzymatic Electrochemical Determination of Dopamine and Uric Acid in presence of Ascorbic Acid
  • 文献类型:   Article
  • 作  者:   BISWAS S, DAS R, CHAKRABORTY D, BANDHYOPADHYAY R, PRAMANIK P
  • 作者关键词:   nitrogen doped graphene, diethanolamine, triethanolamine, electrochemical determination, decomposition of zn complex
  • 出版物名称:   ELECTROANALYSIS
  • ISSN:   1040-0397 EI 1521-4109
  • 通讯作者地址:   MCKV Inst Engn
  • 被引频次:   8
  • DOI:   10.1002/elan.201400617
  • 出版年:   2015

▎ 摘  要

Nitrogen doped multilayered graphene (NDMLG) is synthesized by annealing the black fluffy mass obtained by decomposing the complex prepared from Zn(OAc)(2), diethanolamine and triethanolamine. The NDMLG has been characterized by HRTEM, FESEM, XRD, XPS, Raman spectroscopy, BET which indicate formation of nitrogen doped multilayer graphene flakes with high surface area. NDMLG shows better electrochemical oxidation property towards Dopamine, Uric acid and Ascorbic acid. The linear response ranges for determination of DA, UA and AA are 0.5-150 mu M, 3-60 mu M and 80-2000 mu M respectively and the detection limits (S/N = 3) are 15 nM, 15 nM, 580 nM, respectively in the mixture.