• 文献标题:   Characterization and Properties of Magnetic and Non-magnetic (Gum Acacia/Polyacryamide/Graphene) Nanocomposites Prepared by Gamma Irradiation
  • 文献类型:   Article
  • 作  者:   MAHMOUD GA, ELDIN MRE, SAAD EA, MOHAMED AA
  • 作者关键词:   characterization, graphene, gum acacia, magnetic nanoparticle, nanocomposite
  • 出版物名称:   JOURNAL OF INORGANIC ORGANOMETALLIC POLYMERS MATERIALS
  • ISSN:   1574-1443 EI 1574-1451
  • 通讯作者地址:   Atom Energy Author
  • 被引频次:   0
  • DOI:   10.1007/s10904-018-0901-0
  • 出版年:   2018

▎ 摘  要

Graphene (GR) sheets were successfully prepared via solvent interface trapping. Characterization of GR was performed using Raman spectroscopy, X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), high-resolution transmission electron microscopy (HRTEM), and UV-Vis spectrometer. GR was trapped in gum acacia (GA) and polyacrylamide (PAAm) to form GA/PAAm/GR nanocomposite using gamma irradiation technique. In situ preparation of the magnetic nanocomposite and the magnetization was measured. Characterization the prepared nanocomposites was done using (FT-IR), (FESEM), (HRTEM), (XRD), (TGA). It can be obtained that a high swelling percent was observed for all systems that increased with time until reached the steady state after 5h and the maximum was at pH 10. The swelling percent were ordered in sequence of GA/PAAm-magnetic>GA/PAAm/GR-magnetic>GA/PAAm>GA/PAAm/GR. The thermal stability of the magnetic nanocomposite was higher than non-magnetic one. The mechanical properties were determined using nanoindentation. The elastic modulus and the hardness of GA/PAAm matrix increased by adding GR and GR-magnetic in the nanocomposites.